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Evaluation of the Catalytic Ability of Sulfocationites Based on Petroleum Asphaltenes in the Synthesis of Pyrazolidin-3-one
https://doi.org/10.18412/1816-0387-2020-5-359-365
Abstract
The feasibility of the room temperature catalytic cyclization of hydrazine hydrate and acrylic acid in the presence of an acidic catalyst containing petroleum asphaltenes was explored. The effect of sulfocationite on the synthesis of the target pyrazolidin-3-one was studied. Reaction masses and their distillation residues were analyzed. Gas chromatography–mass spectrometry and electrospray ionization were used to reveal different individual, oligomeric and polymeric products. The most probable structures of the obtained products were proposed.
About the Authors
L. I. Musin
FRC KazSC RAS, Kazan
Russian Federation
Russian Federation
L. E. Foss
FRC KazSC RAS, Kazan
Russian Federation
Russian Federation
K. V. Shabalin
FRC KazSC RAS, Kazan
Russian Federation
Russian Federation
O. A. Nagornova
FRC KazSC RAS, Kazan
Russian Federation
Russian Federation
D. N. Borisov
FRC KazSC RAS, Kazan
Russian Federation
Russian Federation
V. V. Tutuchkina
A.E. Arbuzov Institute of Organic and Physical Chemistry – Subdivision of the Federal State Budgetary Institution of Science «Kazan Scientific Center of Russian Academy of Sciences», Kazan
Russian Federation
Russian Federation
M. R. Yakubov
A.E. Arbuzov Institute of Organic and Physical Chemistry – Subdivision of the Federal State Budgetary Institution of Science «Kazan Scientific Center of Russian Academy of Sciences», Kazan
Russian Federation
Russian Federation
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Review
For citations:
Musin L.I., Foss L.E., Shabalin K.V., Nagornova O.A., Borisov D.N., Tutuchkina V.V., Yakubov M.R. Evaluation of the Catalytic Ability of Sulfocationites Based on Petroleum Asphaltenes in the Synthesis of Pyrazolidin-3-one. Kataliz v promyshlennosti. 2020;20(5):359-365. (In Russ.) https://doi.org/10.18412/1816-0387-2020-5-359-365
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